2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one

Base Information

Chemical Name:2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one
CAS No.:124603-59-4
Molecular Formula:C₂₁H₂₂ClNO₅S
Molecular Weight:435.928
Hs Code.:

Synonyms:2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one

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Chemical Property of 2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one

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Technology Process of 2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one

There total 6 articles about 2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 124603-60-7
3-Chloro-benzoic acid (1S,2S,3R,5R)-2-hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-2-triisopropylsilanyloxy-cyclohexyl ester

: 124603-59-4
2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; for 1h;
DOI:10.1016/0040-4020(95)00696-6

Reference yield:

: 124603-50-5,124603-57-2
trans-6-(4-methylphenylsulfonyl)amino-4-methyl-1-triisopropyl-silyl(oxy)-cyclohex-1-ene

: 124603-59-4
2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaHCO₃ / CH₂Cl₂ / 3 h / 25 °C

2: 95 percent / satd. aq. NaHCO₃ / tetrahydrofuran / 1 h

With sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4020(95)00696-6

Reference yield:

: 937-14-4
3-chloro-benzenecarboperoxoic acid

: 124603-59-4
2α-(4-methylphenylsulfonyl)amino-4β-methyl-6α-(3-chlorobenzoyloxy)-cyclohex-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaHCO₃ / CH₂Cl₂ / 3 h / 25 °C

2: 95 percent / satd. aq. NaHCO₃ / tetrahydrofuran / 1 h

With sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4020(95)00696-6