methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate

Base Information

Chemical Name:methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate
CAS No.:1356601-63-2
Molecular Formula:C₂₉H₃₃NO₅
Molecular Weight:475.585
Hs Code.:

Synonyms:methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate

Suppliers and Price of methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate

There total 9 articles about methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.74%

: 1356601-60-9
methyl 3-(4-hydroxyphenyl)hexanoate

: 1356599-86-4
(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}phenyl)methanol

: 1356601-63-2
methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 16h;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1356601-63-2
methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate

Guidance literature:: Multi-step reaction with 7 steps

1: water / 2 h / 75 °C

2: tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3: water / pentan-3-one / 48 h / Reflux

4: methanesulfonic acid / 2 h / 65 °C

5: potassium carbonate / acetonitrile / 16 h / 0 - 20 °C

6: hydrogen; quinoline / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C

7: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

With quinoline; methanesulfonic acid; di-isopropyl azodicarboxylate; water; hydrogen; potassium carbonate; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; water; ethyl acetate; pentan-3-one; acetonitrile;

Reference yield:

: 865233-34-7
4-hydroxy-β-1-propyn-1-ylbenzenepropanoic acid

: 1356601-63-2
methyl 3-{4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}hexanoate

Guidance literature:: Multi-step reaction with 4 steps

1: methanesulfonic acid / 2 h / 65 °C

2: potassium carbonate / acetonitrile / 16 h / 0 - 20 °C

3: hydrogen; quinoline / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

With quinoline; methanesulfonic acid; di-isopropyl azodicarboxylate; hydrogen; potassium carbonate; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; ethyl acetate; acetonitrile;