methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride

Base Information

Chemical Name:methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride
CAS No.:913652-21-8
Molecular Formula:C₁₆H₁₉ClN₂O₃*ClH
Molecular Weight:359.252
Hs Code.:

Synonyms:methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride

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Chemical Property of methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride

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Technology Process of methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride

There total 7 articles about methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 913652-16-1
2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carbonitrile

: 913652-21-8
methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride

Guidance literature:: methanol; 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carbonitrile; With sodium hydride; at 20 ℃; for 16h;

With hydrogenchloride; In diethyl ether;

Reference yield:

: 913651-30-6
2-((5-chloro-2-[(2-methylpropyl)oxy]phenyl)methyl)-1,3-oxazole-4-carboxylic acid

: 913652-21-8
methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2: trichlorophosphate / 1 h / 75 °C

3: sodium hydride / 16 h / 20 °C

With oxalyl dichloride; sodium hydride; N,N-dimethyl-formamide; trichlorophosphate; In dichloromethane;

Reference yield:

: 26938-87-4
(5-chloro-2-((2-methylpropyl)oxy)phenyl)acetonitrile

: 913652-21-8
methyl 2-({5-chloro-2-[(2-methylpropyl)oxy]phenyl}methyl)-1,3-oxazole-4-carboximidoate hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogenchloride / 2.5 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3: hexamethylenetetramine; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper(ll) bromide / dichloromethane / 0 - 20 °C

4: sodium hydroxide; water / methanol / 1 h / 50 °C

5: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

6: trichlorophosphate / 1 h / 75 °C

7: sodium hydride / 16 h / 20 °C

With hydrogenchloride; sodium hydroxide; oxalyl dichloride; hexamethylenetetramine; water; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; copper(ll) bromide; trichlorophosphate; In methanol; dichloromethane;