4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine

Base Information

• Chemical Name: 4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine
• CAS No.: 124462-58-4
• Molecular Formula: C₁₆H₂₃NO₂Si
• Molecular Weight: 289.45

Synonyms:4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine

Chemical Property of 4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine

Chemical Property:

Purity/Quality:

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Technology Process of 4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine

There total 1 articles about 4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-chloro-1-phenyl-ethanone oxime (21572-32-7) + 1-(trimethylsilyloxy)cyclopentene (19980-43-9) → 4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine (124462-58-4)

Guidance literature:

With sodium carbonate; In diethyl ether; for 94h; Ambient temperature;

Reference yield: 41.0%

4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine (124462-58-4) → 4,5-dihydro-2-phenylcyclopentapyrrole (79379-48-9)

Guidance literature:

With hexacarbonyl molybdenum; trifluoroacetic acid; In acetonitrile; Heating;

Reference yield:

4,4a,5,6,7,7a-hexahydro-3-phenyl-7a-(trimethylsiloxy)cyclopent-1,2-oxazine (124462-58-4) → benzonitrile (100-47-0) + 2-methylenecyclopentanone (1489-50-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

upstream raw materials:

2-chloro-1-phenyl-ethanone oxime

1-(trimethylsilyloxy)cyclopentene

Downstream raw materials:

4,5-dihydro-2-phenylcyclopentapyrrole

benzonitrile

2-methylenecyclopentanone

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