trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride

Base Information

Chemical Name:trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride
CAS No.:1616501-71-3
Molecular Formula:C₂₂H₂₉NO*ClH
Molecular Weight:359.939
Hs Code.:

Synonyms:trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride

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Chemical Property of trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride

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Technology Process of trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride

There total 3 articles about trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1616501-70-2
trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol

: 1616501-71-3
trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride

Guidance literature:: With chloro-trimethyl-silane; In water; butanone;
DOI:10.1021/ml500116x

Reference yield:

: 65619-20-7
4-dimethylamino-4-phenylcyclohexanone

: 1616501-71-3
trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 20 °C

2: chloro-trimethyl-silane / water; butanone

With chloro-trimethyl-silane; In tetrahydrofuran; water; butanone;
DOI:10.1021/ml500116x

Reference yield:

: 65619-92-3
8-(dimethylamino)-1,4-dioxaspiro-[4.5]-decane-8-carbonitrile

: 1616501-71-3
trans-4-dimethylamino-1-phenethyl-4-phenylcylcohexanol hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: hydrogenchloride / water

3.1: tetrahydrofuran / 20 °C

4.1: chloro-trimethyl-silane / water; butanone

With hydrogenchloride; chloro-trimethyl-silane; In tetrahydrofuran; water; butanone; 1.1: |Bruylants Amination;
DOI:10.1021/ml500116x