11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene

Base Information

• Chemical Name: 11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene
• CAS No.: 700375-38-8
• Molecular Formula: C₂₈H₃₂N₂O₇
• Molecular Weight: 508.571

Synonyms:11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene

Chemical Property of 11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene

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Technology Process of 11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene

There total 3 articles about 11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

benzyl bromide (100-39-0) + N-(2-hydroxy-5-nitrobenzyl)benzo-10-aza-15-crown-5 (700375-36-6) → 11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene (700375-38-8)

Guidance literature:

With potassium carbonate; In acetonitrile; for 20h; Heating;

DOI:10.1081/SCC-120030311

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → 11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene (700375-38-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / benzene / 20 h / Heating

2: 92 percent / K₂CO₃ / acetonitrile / 20 h / Heating

With potassium carbonate; In acetonitrile; benzene; 1: Mannich reaction;

DOI:10.1081/SCC-120030311

Reference yield:

benzo-10-aza-15-crown-5 (54533-83-4) → 11-(2-benzyloxy-5-nitro-benzyl)-6,7,10,11,12,13,15,16-octahydro-9H-5,8,14,17-tetraoxa-11-aza-benzocyclopentadecene (700375-38-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / benzene / 20 h / Heating

2: 92 percent / K₂CO₃ / acetonitrile / 20 h / Heating

With potassium carbonate; In acetonitrile; benzene; 1: Mannich reaction;

DOI:10.1081/SCC-120030311

upstream raw materials:

benzyl bromide

N-(2-hydroxy-5-nitrobenzyl)benzo-10-aza-15-crown-5

4-nitro-phenol

benzo-10-aza-15-crown-5

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