10-benzylthio-8-hydrazino-2,2-dimethyl-5-morpholin-4-yl-1,4-dihydro-2H-pyrano-[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

Base Information Edit

Chemical Name:10-benzylthio-8-hydrazino-2,2-dimethyl-5-morpholin-4-yl-1,4-dihydro-2H-pyrano-[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine
CAS No.:1416039-19-4
Molecular Formula:C₂₅H₂₈N₆O₂S₂
Molecular Weight:508.668
Hs Code.:
Mol file:1416039-19-4.mol

Synonyms:10-benzylthio-8-hydrazino-2,2-dimethyl-5-morpholin-4-yl-1,4-dihydro-2H-pyrano-[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

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Chemical Property of 10-benzylthio-8-hydrazino-2,2-dimethyl-5-morpholin-4-yl-1,4-dihydro-2H-pyrano-[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine Edit

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Technology Process of 10-benzylthio-8-hydrazino-2,2-dimethyl-5-morpholin-4-yl-1,4-dihydro-2H-pyrano-[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

There total 2 articles about 10-benzylthio-8-hydrazino-2,2-dimethyl-5-morpholin-4-yl-1,4-dihydro-2H-pyrano-[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 578751-66-3
10-benzylsulfanyl-8-chloro-2,2-dimethyl-5-(morpholin-4-yl)-1,4-dihydro-2H-pyrano[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

: 1416039-19-4
10-benzylthio-8-hydrazino-2,2-dimethyl-5-morpholin-4-yl-1,4-dihydro-2H-pyrano-[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

Guidance literature:: With hydrazine; In isopropyl alcohol; for 5h; Reflux;
DOI:10.1134/S1068162017040070

Reference yield:

: 672341-49-0
10-benzylsulfanyl-2,2-dimethyl-5-(morpholin-4-yl)-1,4-dihydro-2H-pyrano[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8(9H)-one

: 1416039-19-4
10-benzylthio-8-hydrazino-2,2-dimethyl-5-morpholin-4-yl-1,4-dihydro-2H-pyrano-[4'',3'':4',5']pyrido[3',2':4,5]thieno[3,2-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate; pyridine / Heating

2: hydrazine hydrate / isopropyl alcohol / 5 h / Reflux

With pyridine; hydrazine hydrate; trichlorophosphate; In isopropyl alcohol;
DOI:10.1007/s10593-012-1148-2