2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
CAS No.:1615201-42-7
Molecular Formula:C₁₇H₂₀N₂O₄S
Molecular Weight:348.423
Hs Code.:

Synonyms:2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of 2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Chemical Property:

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Technology Process of 2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

There total 4 articles about 2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 879473-33-3
1,2,3,4-tetrahydro-6,7-dimethoxy-2-[(4-nitrophenyl)sulfonyl]isoquinoline

: 1615201-42-7
2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With tin(II) chloride dihdyrate; In ethanol; for 4h; Reflux;
DOI:10.1016/j.ejmech.2014.05.019

Reference yield:

: 321706-24-5
N-[2-(3,4-dimethoxyphenyl)ethyl]-4-nitrobenzenesulfonamide

: 1615201-42-7
2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid / 2 h / 20 °C / Reflux

2: tin(II) chloride dihdyrate / ethanol / 4 h / Reflux

With tin(II) chloride dihdyrate; In formic acid; ethanol; 1: |Pictet-Spengler Synthesis;
DOI:10.1016/j.ejmech.2014.05.019

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 1615201-42-7
2-((4-aminophenyl)sulfonyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / dichloromethane / 20 °C

2: formic acid / Reflux

3: tin(II) chloride dihdyrate / ethanol / Reflux

With tin(II) chloride dihdyrate; sodium carbonate; In formic acid; ethanol; dichloromethane; 2: |Pictet-Spengler Synthesis;
DOI:10.1016/j.bmc.2015.04.036