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Technology Process of V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2]

V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2]

Base Information
  • Chemical Name:V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2]
  • CAS No.:202535-06-6
  • Molecular Formula:C8H20N*C33H43N2O20V4
  • Molecular Weight:1121.73
  • Hs Code.:
V<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CC<sub>2</sub>H<sub>5</sub>)7(C<sub>5</sub>H<sub>4</sub>NCOO)2<sup>(1-)</sup>*N(C<sub>2</sub>H<sub>5</sub>)4<sup>(1+)</sup>=(N(C<sub>2</sub>H<sub>5</sub>)4)[V<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CC<sub>2</sub>H<sub>5</sub>)7(C<sub>5</sub>H<sub>4</sub>NCOO)2]

Synonyms:V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2]

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Chemical Property of V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2]
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Technology Process of V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2]

There total 1 articles about V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

Vanadium (III) chloride-(tris-tetrahydrofuran)
131063-11-1,16997-51-6,19559-06-9

Vanadium (III) chloride-(tris-tetrahydrofuran)

tetraethylammonium chloride
56-34-8

tetraethylammonium chloride

sodium proprionate
137-40-6

sodium proprionate

sodium picolinate
57665-05-1

sodium picolinate

V<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CC<sub>2</sub>H<sub>5</sub>)7(C<sub>5</sub>H<sub>4</sub>NCOO)2<sup>(1-)</sup>*N(C<sub>2</sub>H<sub>5</sub>)4<sup>(1+)</sup>=(N(C<sub>2</sub>H<sub>5</sub>)4)[V<sub>4</sub>O<sub>2</sub>(O<sub>2</sub>CC<sub>2</sub>H<sub>5</sub>)7(C<sub>5</sub>H<sub>4</sub>NCOO)2]
202535-06-6

V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2]

sodium chloride
7647-14-5

sodium chloride

Guidance literature:
In acetonitrile; inert atmosphere, Schlenk techniques; aq. Na(pic) soln. addn. to stirred mixt. of V-compd., NaO2CEt and MeCN, stirring overnight, NaCl ppt. filtration off, NEt4Cl addn. to filtrate, solvent removal (vac.), residue redissoln. (acetone), THF addn.; pptn. after a few on standing at room temp., ppt. filtration off, washing (THF), vac. drying; elem. anal.;
DOI:10.1021/ja9732439
upstream raw materials:

Vanadium (III) chloride-(tris-tetrahydrofuran)

tetraethylammonium chloride

sodium proprionate

sodium picolinate

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