10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate

Base Information

Chemical Name:10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate
CAS No.:327168-35-4
Molecular Formula:C₁₄H₁₉N₅S
Molecular Weight:289.404
Hs Code.:

Synonyms:10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate

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Chemical Property of 10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate

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Technology Process of 10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate

There total 1 articles about 10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 5355-68-0
1-Isopropyl-4-piperidone

: 7357-70-2
Cyanothioacetamide

: 109-77-3
malononitrile

: 327168-35-4
10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate

Guidance literature:: In ethanol; at 20 ℃; for 2h;
DOI:10.1080/10426500902855075

Reference yield: 79.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 327168-35-4
10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate

: 108-44-1
1-amino-3-methylbenzene

: 1105690-34-3
1'-isopropyl-5,11-di(3-methylphenyl)-8-thioxospiro[3,5,7,11-tetraazatricyclo[7.3.1.0^2,7]tridec-2-ene-13,4'-piperidine]-1,9-dicarbonitrile

Guidance literature:: formaldehyd; 10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate; 1-amino-3-methylbenzene; In ethanol; for 0.05h; Heating;

In ethanol; at -20 ℃; for 8h; Further stages.;
DOI:10.1007/s10593-007-0224-5

Reference yield: 77.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 327168-35-4
10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate

: 62-53-3
aniline

: 1105690-29-6
1'-isopropyl-5,11-diphenyl-8-thioxospiro[3,5,7,11-tetraazatricyclo[7.3.1.0^2,7]tridec-2-ene-piperidine]-1,9-dicarbonitrile

Guidance literature:: formaldehyd; 10-amino-9-aza-3-azonia-7,11-dicyano-3-isopropylspiro[5,5]undeca-7,10-diene-8-thiolate; aniline; In ethanol; for 0.05h; Heating;

In ethanol; at -20 ℃; for 8h; Further stages.;
DOI:10.1007/s10593-007-0224-5