1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione

Base Information

Chemical Name:1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione
CAS No.:343338-99-8
Molecular Formula:C₁₆H₁₁F₃O₅
Molecular Weight:340.256
Hs Code.:

Synonyms:1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione

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Chemical Property of 1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione

Chemical Property:

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Technology Process of 1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione

There total 3 articles about 1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 343338-98-7
4-(furan-2-yl)-3-(methoxycarbonyl)phenyl-1-ethanone

: 383-63-1
ethyl trifluoroacetate,

: 343338-99-8
1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione

Guidance literature:: With sodium methylate; In 1,2-dimethoxyethane; at 20 ℃;
DOI:10.1016/j.bmcl.2006.01.059

Reference yield:

: 16475-90-4
estere metilico dell'acido 5-acetilsalicilico

: 343338-99-8
1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / -40 °C

2: Pd(PPh₃)4; LiCl / dioxane / 110 °C

3: NaOMe / 1,2-dimethoxy-ethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium methylate; triethylamine; lithium chloride; In 1,4-dioxane; 1,2-dimethoxyethane; 3: Claisen condensation;
DOI:10.1016/j.bmcl.2006.01.059

Reference yield:

: 343338-97-6
5-acetyl-2-(trifluoro-methyl-sulfonyloxy)-benzoic acid,methyl ester

: 343338-99-8
1-[4-(2-Furyl)3-(methoxycarbonyl)phenyl]-4,4,4-trifluoro-1,3-butanedione

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(PPh₃)4; LiCl / dioxane / 110 °C

2: NaOMe / 1,2-dimethoxy-ethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium methylate; lithium chloride; In 1,4-dioxane; 1,2-dimethoxyethane; 2: Claisen condensation;
DOI:10.1016/j.bmcl.2006.01.059