2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid

Base Information

Chemical Name:2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid
CAS No.:1362820-33-4
Molecular Formula:C₂₂H₁₇BrO₅
Molecular Weight:441.278
Hs Code.:

Synonyms:2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid

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Chemical Property of 2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid

Chemical Property:

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Technology Process of 2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid

There total 8 articles about 2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1362819-85-9
phenylmethyl 5-bromo-4-formyl-2-[(phenylmethyl)oxy]benzoate

: 1362820-33-4
2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid

Guidance literature:: With sodium chlorite; aminosulfonic acid; 2-Methyl-1-butene; In tetrahydrofuran; water; dimethyl sulfoxide; at 0 ℃; for 0.75h;

Reference yield:

: 50-85-1
2-hydroxy-p-toluic acid

: 1362820-33-4
2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / 24 h / 50 °C

2: bromine / chloroform / 1 h / 0 °C

3: pyridine / 4 h

4: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 85 °C

5: water; calcium carbonate / 1,4-dioxane / 3 h / 150 °C

6: potassium carbonate / N,N-dimethyl-formamide / 21 h / 50 °C

7: 2-Methyl-1-butene; aminosulfonic acid; sodium chlorite / water; dimethyl sulfoxide; tetrahydrofuran / 0.75 h / 0 °C

With pyridine; sodium chlorite; N-Bromosuccinimide; thionyl chloride; aminosulfonic acid; water; bromine; potassium carbonate; 2-Methyl-1-butene; calcium carbonate; dibenzoyl peroxide; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 4670-56-8
methyl 2-hydroxy-4-methylbenzoate

: 1362820-33-4
2-bromo-5-[(phenylmethyl)oxy]-4-{[(phenylmethyl)oxy]carbonyl}benzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / chloroform / 1 h / 0 °C

2: pyridine / 4 h

3: N-Bromosuccinimide / dibenzoyl peroxide / tetrachloromethane / 85 °C

4: water; calcium carbonate / 1,4-dioxane / 3 h / 150 °C

5: potassium carbonate / N,N-dimethyl-formamide / 21 h / 50 °C

6: 2-Methyl-1-butene; aminosulfonic acid; sodium chlorite / water; dimethyl sulfoxide; tetrahydrofuran / 0.75 h / 0 °C

With pyridine; sodium chlorite; N-Bromosuccinimide; aminosulfonic acid; water; bromine; potassium carbonate; 2-Methyl-1-butene; calcium carbonate; dibenzoyl peroxide; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide;