N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide

Base Information

• Chemical Name: N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide
• CAS No.: 1215009-04-3
• Molecular Formula: C₁₅H₂₁N₃O₃S
• Molecular Weight: 323.416

Synonyms:N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide

Chemical Property of N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide

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Technology Process of N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide

There total 1 articles about N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

4-amino-3,5-dimethyl-1H-pyrazole (5272-86-6) + 4-methoxy-2,3,6-trimethylbenzenesulfonyl chloride (80745-07-9) → N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide (1215009-04-3)

Guidance literature:

With pyridine; at 20 ℃;

DOI:10.1021/jm201091t

Reference yield: 24.0%

N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide (1215009-04-3) + propyl bromide (106-94-5) → N-(1-propyl-3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide (1215009-84-9)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1h; Microwave irradiation;

DOI:10.1021/jm201091t

Reference yield: 19.0%

N-(3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide (1215009-04-3) + isopropyl bromide (75-26-3) → N-(1-isopropyl-3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide (1215009-90-7)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; Microwave irradiation;

DOI:10.1021/jm201091t

upstream raw materials:

4-amino-3,5-dimethyl-1H-pyrazole

4-methoxy-2,3,6-trimethylbenzenesulfonyl chloride

Downstream raw materials:

N-(1-propyl-3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide

N-(1-isopropyl-3,5-dimethyl-1H-pyrazol-4-yl)-4-methoxy-2,3,6-trimethylbenzenesulfonamide

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