Technology Process of C24H36O4
There total 9 articles about C24H36O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
5%-palladium/activated carbon; hydrogen;
In
ethanol;
at 30 ℃;
for 3h;
under 760.051 Torr;
DOI:10.1002/adsc.201100898
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap; iodine; potassium carbonate / tetrahydrofuran; water / 2 h / 20 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride / 1,2-dimethoxyethane; water / 12 h / 80 °C / Inert atmosphere
3: 5%-palladium/activated carbon; hydrogen / ethanol / 3 h / 30 °C / 760.05 Torr
With
dmap; tetrakis(triphenylphosphine) palladium(0); 5%-palladium/activated carbon; hydrogen; iodine; sodium carbonate; potassium carbonate; lithium chloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water;
2: Suzuki coupling;
DOI:10.1002/adsc.201100898
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: bromine / acetic acid / 4 h / 20 °C
2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 1.5 h / -78 - -30 °C / Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride / 1,2-dimethoxyethane; water / 12 h / 80 °C / Inert atmosphere
4.1: 5%-palladium/activated carbon; hydrogen / ethanol / 3 h / 30 °C / 760.05 Torr
With
tetrakis(triphenylphosphine) palladium(0); n-butyllithium; 5%-palladium/activated carbon; hydrogen; bromine; sodium carbonate; lithium chloride;
In
tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; acetic acid;
3.1: Suzuki coupling;
DOI:10.1002/adsc.201100898