t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate

Base Information

Chemical Name:t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate
CAS No.:1227157-26-7
Molecular Formula:C₁₇H₁₇ClN₂O₄
Molecular Weight:348.786
Hs Code.:

Synonyms:t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate

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Chemical Property of t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate

Chemical Property:

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Technology Process of t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate

There total 5 articles about t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 49609-84-9
2-Chloronicotinoyl chloride

: 95932-39-1
carbonic acid 4-aminophenyl ester tert-butyl ester

: 1227157-26-7
t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 12h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1227157-26-7
t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / dichloromethane / 10 h / 20 °C

2: hydrogen / palladium / ethyl acetate / 24 h / 20 °C

3: triethylamine / dichloromethane / 12 h / 0 - 20 °C

With dmap; hydrogen; triethylamine; palladium; In dichloromethane; ethyl acetate;

Reference yield:

: 13303-10-1
tert-Butyl 4-nitrophenyl carbonate

: 1227157-26-7
t-butyl 4-(2-chloro-nicotine amino)phenyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium / ethyl acetate / 24 h / 20 °C

2: triethylamine / dichloromethane / 12 h / 0 - 20 °C

With hydrogen; triethylamine; palladium; In dichloromethane; ethyl acetate;