6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

Base Information

Chemical Name:6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one
CAS No.:1186017-09-3
Molecular Formula:C₃₉H₄₇N₃O₉S
Molecular Weight:733.883
Hs Code.:

6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

Synonyms:6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

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Chemical Property of 6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

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Technology Process of 6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

There total 6 articles about 6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 911705-03-8
2,2,2-trichloro-acetimidic acid 4-(3-methoxy-propyl)-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethyl ester

: 1186017-10-6
(S)-4-benzyl-3-{(S,R)-3-[(2S,5R)-5-hydroxy-1-(toluene-4-sulphonyl)piperidin-2-yl]-2-methylpropionyl}oxazolidin-2-one

: 1186017-09-3
6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

Guidance literature:: scandium tris(trifluoromethanesulfonate); In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 1186017-11-7
(S)-4-benzyl-3-{(S,R)-3-[(2S,5R)-5-(4-methoxy-benzyloxy)-1-(toluene-4-sulphonyl)piperidin-2-yl]-2-methylpropionyl}oxazolidin-2-one

: 1186017-09-3
6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / 5%-palladium/activated carbon / tetrahydrofuran; methanol / 760.05 Torr

2: scandium tris(trifluoromethanesulfonate) / dichloromethane / 2 h / 0 °C

With hydrogen; 5%-palladium/activated carbon; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 857272-03-8
6-hydroxymethyl-4-(3-methoxy-propyl)-4H-benzo[1,4]oxazin-3-one

: 1186017-09-3
6-[(3R,6S)-6-[3-((S)-4-benzyl-2-oxo-oxazolidin-3-yl)-2-methyl-3-oxopropyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy-methyl]-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / dichloromethane; water / 2 h / 0 - 20 °C

2: scandium tris(trifluoromethanesulfonate) / dichloromethane / 2 h / 0 °C

With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; scandium tris(trifluoromethanesulfonate); In dichloromethane; water;