N,N'-di(p-tolylsulfonyl)selenium diimide

Base Information

• Chemical Name: N,N'-di(p-tolylsulfonyl)selenium diimide
• CAS No.: 60123-29-7
• Molecular Formula: C₁₄H₁₄N₂O₄S₂Se
• Molecular Weight: 417.368

Synonyms:N,N'-di(p-tolylsulfonyl)selenium diimide

Chemical Property of N,N'-di(p-tolylsulfonyl)selenium diimide

Chemical Property:

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Technology Process of N,N'-di(p-tolylsulfonyl)selenium diimide

There total 2 articles about N,N'-di(p-tolylsulfonyl)selenium diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroamine-T (127-65-1) → N,N'-di(p-tolylsulfonyl)selenium diimide (60123-29-7)

Guidance literature:

With selenium; In dichloromethane; for 24h;

Reference yield:

toluene-4-sulfonamide (70-55-3) → N,N'-di(p-tolylsulfonyl)selenium diimide (60123-29-7)

Guidance literature:

With selenium tetrachloride; triethylamine; In dichloromethane-d2; for 1h; Inert atmosphere;

DOI:10.1021/jacs.0c06997

Reference yield: 88.0%

N,N'-di(p-tolylsulfonyl)selenium diimide (60123-29-7) + isoprene (78-79-5,9003-31-0) → 4-Methyl-N-[5-methyl-2-(toluene-4-sulfonyl)-3,6-dihydro-2H-1λ4-[1,2]selenazin-(1E)-ylidene]-benzenesulfonamide (108223-49-0)

Guidance literature:

In diethyl ether; at 20 ℃; for 2h;

upstream raw materials:

chloroamine-T

toluene-4-sulfonamide

Downstream raw materials:

4-methyl-N-(3-caren-10-yl)benzenesulfonamide

(1S,2S,6R)-4-methyl-N-trans-(3-caren-2-yl)benzenesulfonamide

trans-6-(4-methylphenylsulfonyl)amino-4-methyl-1-triisopropyl-silyl(oxy)-cyclohex-1-ene

N-((1S,6R)-6-Isopropenyl-3-methyl-2-triisopropylsilanyloxy-cyclohex-2-enyl)-4-methyl-benzenesulfonamide

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