3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene

Base Information

Chemical Name:3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene
CAS No.:155312-78-0
Molecular Formula:C₂₉H₃₅F₃O₄SSi
Molecular Weight:564.741
Hs Code.:

Synonyms:3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene

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Chemical Property of 3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene

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Technology Process of 3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene

There total 6 articles about 3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 155312-77-9
3-tert-butyldiphenylsilyloxymethyl-3-(4-oxopentyl)-1,4-cyclohexadiene

: 155312-78-0
3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 - 0 ℃; 1.) 40 min; 2.) 1 h;

Reference yield:

: 3695-28-1
5-iodo-2-pentanone ethylene ketal

: 155312-78-0
3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / LDA / tetrahydrofuran / 1 h / 0 °C

2: LiAlH₄ / diethyl ether / 1 h / 0 °C

3: imidazole / dimethylformamide / 1 h / 23 °C

4: 80 percent / 1.) LDA / tetrahydrofuran / -78 - 0 °C / 1.) 40 min; 2.) 1 h

With 1H-imidazole; lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 30889-20-4
methyl cyclohexa-2,5-diene-1-carboxylate

: 155312-78-0
3-tert-butyldiphenylsilyloxymethyl-3-(4-trifluoromethanesulfonyloxy-4-pentenyl)-1,4-cyclohexadiene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / LDA / tetrahydrofuran / 1 h / 0 °C

2: LiAlH₄ / diethyl ether / 1 h / 0 °C

3: imidazole / dimethylformamide / 1 h / 23 °C

4: 80 percent / 1.) LDA / tetrahydrofuran / -78 - 0 °C / 1.) 40 min; 2.) 1 h

With 1H-imidazole; lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;