Technology Process of 4-benzylphenyl tosylate
There total 2 articles about 4-benzylphenyl tosylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis(1,5-cyclooctadiene)nickel (0); 1,8-diazabicyclo[5.4.0]undec-7-ene; trimethylphosphane;
In
tetrahydrofuran;
at 110 ℃;
for 12h;
chemoselective reaction;
Inert atmosphere;
DOI:10.1021/acscatal.8b01224
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine hydrate / tetrahydrofuran / 0.5 h / 20 °C
2: bis(1,5-cyclooctadiene)nickel (0); trimethylphosphane; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 12 h / 110 °C / Inert atmosphere
With
bis(1,5-cyclooctadiene)nickel (0); hydrazine hydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trimethylphosphane;
In
tetrahydrofuran;
DOI:10.1021/acscatal.8b01224
- Guidance literature:
-
4-benzylphenyl tosylate;
With
bis(1,5-cyclooctadiene)nickel (0); 1,8-diazabicyclo[5.4.0]undec-7-ene; trimethylphosphane;
In
tetrahydrofuran;
at 110 ℃;
for 12h;
Inert atmosphere;
(furan-2-ylmethylidene)hydrazine;
In
tetrahydrofuran;
chemoselective reaction;
DOI:10.1021/acscatal.8b01224
