[(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

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Chemical Name:[(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester
CAS No.:247017-97-6
Molecular Formula:C₃₈H₃₄IN₃O₅
Molecular Weight:739.61
Hs Code.:

Synonyms:[(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

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Chemical Property of [(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

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Technology Process of [(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

There total 3 articles about [(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 247017-96-5
[(R)-2-[1-(2-Chloromethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

: 247017-97-6
[(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

Guidance literature:: With sodium iodide; In acetone; Heating;
DOI:10.1016/S0960-894X(00)00183-9

Reference yield:

: 42908-86-1
2-Chloromethylbenzoyl chloride

: 247017-97-6
[(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: KN(TMS)2 / tetrahydrofuran / -78 °C

1.2: 99 percent / tetrahydrofuran

2.1: 100 percent / NaI / acetone / Heating

With potassium hexamethylsilazane; sodium iodide; In tetrahydrofuran; acetone; 1.1: Metallation / 1.2: Acylation / 2.1: Iodination;
DOI:10.1016/S0960-894X(00)00183-9

Reference yield:

: 158991-23-2
PD 154075

: 247017-97-6
[(R)-2-[1-(2-Iodomethyl-benzoyl)-1H-indol-3-yl]-1-methyl-1-((S)-1-phenyl-ethylcarbamoyl)-ethyl]-carbamic acid benzofuran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: KN(TMS)2 / tetrahydrofuran / -78 °C

1.2: 99 percent / tetrahydrofuran

2.1: 100 percent / NaI / acetone / Heating

With potassium hexamethylsilazane; sodium iodide; In tetrahydrofuran; acetone; 1.1: Metallation / 1.2: Acylation / 2.1: Iodination;
DOI:10.1016/S0960-894X(00)00183-9