1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide

Base Information

Chemical Name:1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide
CAS No.:1429476-95-8
Molecular Formula:C₁₇H₁₆F₃NO₅S
Molecular Weight:403.379
Hs Code.:

Synonyms:1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide

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Chemical Property of 1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide

Chemical Property:

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Technology Process of 1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide

There total 3 articles about 1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1159505-53-9
N-(2-methoxybenzyl)triflamide

: 105-13-5
4-Methoxybenzyl alcohol

: 1429476-95-8
1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide

Guidance literature:: With tert.-butylhydroperoxide; palladium diacetate; acetic acid; In decane; acetonitrile; at 120 ℃; for 40h; Sealed tube;
DOI:10.1039/c3ob40140e

Reference yield: 71.0%

: 1159505-53-9
N-(2-methoxybenzyl)triflamide

: 123-11-5
4-methoxy-benzaldehyde

: 1429476-95-8
1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide

Guidance literature:: With tert.-butylhydroperoxide; palladium diacetate; acetic acid; In N,N-dimethyl-formamide; acetonitrile; at 100 ℃; for 40h; Reagent/catalyst; Solvent; Inert atmosphere; Sealed tube;
DOI:10.1002/adsc.201200889

Reference yield:

: 1159505-53-9
N-(2-methoxybenzyl)triflamide

: 123-11-5
4-methoxy-benzaldehyde

: 66-25-1
hexanal

: 1429476-95-8
1,1,1-trifluoro-N-(2-methoxy-6-(4-methoxybenzoyl)benzyl)methanesulfonamide

: 1429477-03-1
1,1,1-trifluoro-N-(2-methoxy-6-(hexanoyl)benzyl)methanesulfonamide

Guidance literature:: With tert.-butylhydroperoxide; palladium diacetate; acetic acid; In N,N-dimethyl-formamide; acetonitrile; at 100 ℃; for 40h; Overall yield = 62 %; Inert atmosphere; Sealed tube;
DOI:10.1002/adsc.201200889