C₉H₉ClO

Base Information

• Chemical Name: C₉H₉ClO
• CAS No.: 854673-32-8
• Molecular Formula: C₉H₉ClO
• Molecular Weight: 168.623
• Mol file: 854673-32-8.mol

Synonyms:C₉H₉ClO

Chemical Property of C₉H₉ClO

Chemical Property:

Purity/Quality:

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Technology Process of C₉H₉ClO

There total 1 articles about C₉H₉ClO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

β-chlorocinnamaldehyde (33603-87-1,49633-86-5,40133-53-7) → C9H9ClO (854673-32-8)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1002/chem.200601418

Reference yield: 67.0%

C9H9ClO (854673-32-8) + N-fluorobis(benzenesulfon)imide (133745-75-2) → N-(1-chloro-3-hydroxy-1-phenylpropan-2-yl)-N-(phenylsulfonyl)benzenesulfonamide

Guidance literature:

With copper dichloride; In acetonitrile; at 60 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.201801262

Reference yield:

C9H9ClO (854673-32-8) + methanesulfonyl chloride (124-63-0) → C10H11ClO3S

Guidance literature:

With triethylamine; In diethyl ether; at 0 ℃; for 0.5h;

DOI:10.1021/acs.orglett.0c03865

upstream raw materials:

β-chlorocinnamaldehyde