(2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid

Base Information

Chemical Name:(2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid
CAS No.:575457-75-9
Molecular Formula:C₂₄H₁₉N₅O₉
Molecular Weight:521.443
Hs Code.:

Synonyms:(2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid

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Chemical Property of (2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid

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Technology Process of (2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid

There total 11 articles about (2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 575457-73-7
C₂₄H₂₁N₅O₈

: 3240-34-4
[bis(acetoxy)iodo]benzene

: 575457-75-9
(2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In water; acetonitrile; at 20 ℃; for 6h;

Reference yield:

: 575457-73-7
C₂₄H₂₁N₅O₈

: 575457-75-9
(2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; water; In acetonitrile; at 20 ℃; for 4h;
DOI:10.1021/ol0507322

Reference yield:

: 575457-72-6
C₂₆H₂₃N₅O₉

: 575457-75-9
(2S,3S,4S,5R,6R)-3-Azido-4,5-bis-benzoyloxy-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-pyran-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / methanol / 24 h / 20 °C

2: 1.2 g / H₂O; TEMPO; iodobenzene diacetate / acetonitrile / 4 h / 20 °C

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene; water; triethylamine; In methanol; acetonitrile;
DOI:10.1021/ol0507322