1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline

Base Information

Chemical Name:1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline
CAS No.:79832-10-3
Molecular Formula:C₂₁H₂₄N₂O₇
Molecular Weight:416.431
Hs Code.:

Synonyms:1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline

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Chemical Property of 1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline

Chemical Property:

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Technology Process of 1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline

There total 4 articles about 1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 79831-93-9
4,5-dimethoxy-2-nitro-N-(3,4,5-trimethoxyphenethyl)phenylacetamide

: 79832-10-3
1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline

Guidance literature:: With trichlorophosphate; In chloroform; for 0.416667h; Heating;
DOI:10.1039/P19810002002

Reference yield:

: 54-04-6
mescaline

: 79832-10-3
1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogen carbonate / CHCl₃; diethyl ether; H₂O / 0.25 h

2: 81 percent / phosphorus oxychloride / CHCl₃ / 0.42 h / Heating

With sodium hydrogencarbonate; trichlorophosphate; In diethyl ether; chloroform; water;
DOI:10.1039/P19810002002

Reference yield:

: 73357-18-3
(4,5-dimethoxy-2-nitrophenyl)acetic acid

: 79832-10-3
1-(4,5-dimethoxy-2-nitrobenzyl)-3,4-dihydro-6,7,8-trimethoxyisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, dimethylformamide / benzene / 20 °C

2: sodium hydrogen carbonate / CHCl₃; diethyl ether; H₂O / 0.25 h

3: 81 percent / phosphorus oxychloride / CHCl₃ / 0.42 h / Heating

With oxalyl dichloride; sodium hydrogencarbonate; N,N-dimethyl-formamide; trichlorophosphate; In diethyl ether; chloroform; water; benzene;
DOI:10.1039/P19810002002