[(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate

Base Information

Chemical Name:[(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate
CAS No.:1613396-53-4
Molecular Formula:C₂₁H₂₄ClF₃N₆O₄S
Molecular Weight:548.974
Hs Code.:

Synonyms:[(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate

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Chemical Property of [(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate

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Technology Process of [(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate

There total 12 articles about [(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613396-51-2
(2S)-N-[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]-4-hydroxy-2-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]butanamide

: 124-63-0
methanesulfonyl chloride

: 1613396-53-4
[(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 10 ℃; for 0.5h;

Reference yield:

: 1613396-41-0
(3S)-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]tetrahydrofuran-2-one

: 1613396-53-4
[(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylaluminum / 1,2-dichloro-ethane; toluene / 0 - 20 °C

2: triethylamine / dichloromethane / 0.5 h / 0 - 10 °C

With trimethylaluminum; triethylamine; In dichloromethane; 1,2-dichloro-ethane; toluene;

Reference yield:

: C₁₈H₂₁F₃N₂O₃

: 1613396-53-4
[(3S)-4-[[1-(4-chlorophenyl)-5-isopropyl-triazol-4-yl]amino]-3-[2-methyl-4-(trifluoromethyl)imidazol-1-yl]-4-oxo-butyl]methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 1,4-dioxane / 1 h / 80 °C

2: trimethylaluminum / 1,2-dichloro-ethane; toluene / 0 - 20 °C

3: triethylamine / dichloromethane / 0.5 h / 0 - 10 °C

With sulfuric acid; trimethylaluminum; triethylamine; In 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane; toluene;