N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

Base Information

Chemical Name:N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine
CAS No.:438036-76-1
Molecular Formula:C₄₆H₄₃NO₆
Molecular Weight:705.851
Hs Code.:

Synonyms:N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

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Chemical Property of N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

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Technology Process of N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

There total 1 articles about N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 15778-71-9
N-(4-benzyloxy-3-methoxybenzyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

: 438036-76-1
N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

Guidance literature:: With sodium carbonate; In tetrahydrofuran; water; at 0 ℃; for 5h;
DOI:10.1021/jo020010d

Reference yield: 85.0%

: 438036-76-1
N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

: 438036-75-0
N-(4-hydroxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-hydroxy-3-methoxyphenyl)ethyl)amine

Guidance literature:: With hydrogen; 10percent Pd/C; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo020010d

Reference yield:

: 438036-76-1
N-(4-benzyloxy-3-methoxybenzyl)-N-(9-fluorenylmethyloxycarbonyl)-N-(2-(4-benzyloxy-3-methoxyphenyl)ethyl)amine

: N-(4-hydroxy-5-methoxy-2-piperidinobenzyl)-6-hydroxy-5-methoxyindole

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 20 °C

2: 93 percent / CH₂Cl₂ / -78 °C

3: 21 percent / CH₂Cl₂ / 1.17 h / 0 - 20 °C

With hydrogen; 10percent Pd/C; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo020010d