[[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane

Base Information

• Chemical Name: [[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane
• CAS No.: 1021491-55-3
• Molecular Formula: C₁₅H₂₄O₃Si
• Molecular Weight: 280.439

Synonyms:[[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane

Chemical Property of [[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane

Chemical Property:

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Technology Process of [[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane

There total 1 articles about [[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

chloro-trimethyl-silane (75-77-4) + 2-(1-methyl-1-phenylethoxy)acetic acid methyl ester (1021491-75-7) → [[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane (1021491-55-3)

Guidance literature:

2-(1-methyl-1-phenylethoxy)acetic acid methyl ester; With potassium hexamethylsilazane; In tetrahydrofuran; at -78 - -70 ℃; for 0.5h;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - -70 ℃; for 1.08333h; Further stages.;

DOI:10.1021/jo8006539

Reference yield: 99.0%

4-Trifluoromethylbenzaldehyde (455-19-6) + [[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane (1021491-55-3) → (2R,3S)-3-hydroxy-2-(1-methyl-1-phenylethoxy)-3-[4-(trifluoromethyl)phenyl]propanoic acid methyl ester (1021491-62-2)

Guidance literature:

With tetrachlorosilane; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 0.5h;

DOI:10.1021/jo8006539

Reference yield: 94.0%

[[(Z)-1-methoxy-2-(1-methyl-1-phenylethoxy)ethenyl]oxy](trimethyl)silane (1021491-55-3) + β-naphthaldehyde (66-99-9) → (2R,3S)-3-hydroxy-2-(1-methyl-1-phenylethoxy)-3-(2-naphthyl)propanoic acid methyl ester (1021491-64-4)

Guidance literature:

With tetrachlorosilane; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 0.5h;

DOI:10.1021/jo8006539

upstream raw materials:

chloro-trimethyl-silane

2-(1-methyl-1-phenylethoxy)acetic acid methyl ester

Downstream raw materials:

(2R,3S)-3-hydroxy-2-(1-methyl-1-phenylethoxy)-3-[4-(trifluoromethyl)phenyl]propanoic acid methyl ester

(2R,3S)-3-hydroxy-3-(4-methylphenyl)-2-(1-methyl-1-phenylethoxy)propanoic acid methyl ester

(2R,3S)-3-hydroxy-3-(4-chlorophenyl)-2-(1-methyl-1-phenylethoxy)propanoic acid methyl ester

(2R,3S)-3-hydroxy-2-(1-methyl-1-phenylethoxy)-3-(1-naphthyl)propanoic acid methyl ester

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