(S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate

Base Information

Chemical Name:(S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate
CAS No.:1489278-81-0
Molecular Formula:C₂₈H₃₂N₂O₄S
Molecular Weight:492.639
Hs Code.:

Synonyms:(S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate

Suppliers and Price of (S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate

There total 7 articles about (S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₄N₂O₄S

: 1489278-81-0
(S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; toluene; at 50 ℃; for 2h;
DOI:10.1016/j.ejmech.2013.09.017

Reference yield:

: 1489290-63-2
C₂₅H₃₀N₂O₄S

: 1489278-81-0
(S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / toluene; dimethyl sulfoxide / 2 h / 50 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C

2.2: 4 h / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / toluene; dimethyl sulfoxide / 2 h / 50 °C

With lithium aluminium tetrahydride; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.ejmech.2013.09.017

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 1489278-81-0
(S,E)-tert-butyl 2-(4-(benzyloxy)phenyl)-1-(5-methyl-4-(2-methyl-3-oxoprop-1-enyl)thiazol-2-yl)ethylcarbamate

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; triethylamine / dichloromethane / 2 h / 20 °C

2.1: Lawessons reagent / tetrahydrofuran / 2 h / 65 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / toluene; dimethyl sulfoxide / 2 h / 50 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C

5.2: 4 h / 20 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C

7.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / toluene; dimethyl sulfoxide / 2 h / 50 °C

With Lawessons reagent; dmap; lithium aluminium tetrahydride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.ejmech.2013.09.017