α-Formyloxy cyclohexanone

Base Information

• Chemical Name: α-Formyloxy cyclohexanone
• CAS No.: 80248-49-3
• Molecular Formula: C₇H₁₀O₃
• Molecular Weight: 142.155
• Mol file: 80248-49-3.mol

Synonyms:α-Formyloxy cyclohexanone

Chemical Property of α-Formyloxy cyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-Formyloxy cyclohexanone

There total 3 articles about α-Formyloxy cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

formic acid (64-18-6) + cyclohexanone-2-ol (533-60-8) → α-Formyloxy cyclohexanone (80248-49-3)

Guidance literature:

With acetic anhydride;

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → α-Formyloxy cyclohexanone (80248-49-3) + cyclohexanone-2-ol (533-60-8)

Guidance literature:

cyclohexanone; N,N-dimethyl-formamide; With trifluorormethanesulfonic acid; thallium(III) acetate; at 60 ℃; for 0.333333h;

With water; for 0.166667h; Further stages. Title compound not separated from byproducts.;

DOI:10.1039/b102192n

Reference yield:

formyl fluoride (1493-02-3) + cyclohexanone-2-ol (533-60-8) → α-Formyloxy cyclohexanone (80248-49-3)

Guidance literature:

With pyridine;

DOI:10.1139/v63-303

upstream raw materials:

formyl fluoride

cyclohexanone-2-ol

formic acid

cyclohexanone