Technology Process of C40H50FNO7
There total 6 articles about C40H50FNO7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: boron tribromide / dichloromethane / -30 - 25 °C
2.1: boron trifluoride diethyl etherate / 0.25 h / Reflux
3.1: hydrogenchloride / 0.75 h / -10 - 0 °C
4.1: piperidine / benzene / 16 h / Dean-Stark; Reflux
5.1: caesium carbonate / acetone / 0.17 h / 0 °C
5.2: 19 h / 60 °C
6.1: tetrahydrofuran / 6 h / -5 - 25 °C
With
piperidine; hydrogenchloride; boron trifluoride diethyl etherate; boron tribromide; caesium carbonate;
In
tetrahydrofuran; dichloromethane; acetone; benzene;
- Guidance literature:
-
In
tetrahydrofuran;
at -5 - 25 ℃;
for 6h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: boron trifluoride diethyl etherate / 0.25 h / Reflux
2.1: hydrogenchloride / 0.75 h / -10 - 0 °C
3.1: piperidine / benzene / 16 h / Dean-Stark; Reflux
4.1: caesium carbonate / acetone / 0.17 h / 0 °C
4.2: 19 h / 60 °C
5.1: tetrahydrofuran / 6 h / -5 - 25 °C
With
piperidine; hydrogenchloride; boron trifluoride diethyl etherate; caesium carbonate;
In
tetrahydrofuran; acetone; benzene;