(1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

Base Information

Chemical Name:(1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid
CAS No.:1246818-17-6
Molecular Formula:C₂₈H₃₂F₂N₂O₃S
Molecular Weight:514.636
Hs Code.:

(1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

Synonyms:(1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

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Chemical Property of (1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

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Technology Process of (1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

There total 1 articles about (1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1246818-17-6
(1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

Guidance literature:

Reference yield:

: 38870-89-2
Methoxyacetyl chloride

: 1246818-17-6
(1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

: 1246818-02-9
(1R,3aS,3bS,5S,10aR,10bS,11S,12aS)-7-(6-fluoropyridin-3-yl)-11-hydroxy-1-[(methoxyacetyl)oxy]-10a,12a-dimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

Guidance literature:: Methoxyacetyl chloride; (1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid; With triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;

With N'-ethyl-N,N-dimethyl-1,2-ethanediamine; In dichloromethane; for 0.166667h;

Reference yield:

: 1246818-17-6
(1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

: 79-03-8
propionyl chloride

: 1246817-94-6
(1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(6-fluoropyridin-3-yl)-11-hydroxy-2,10a,12a-trimethyl-1-(propanoyloxy)-1,2,3,3 a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid

Guidance literature:: (1R,2R,3aS,3bS,10aS,10bR,11S,12aS)-10b-fluoro-7-(4-fluorophenyl)-1,11-dihydroxy-2,10a,12a-trimethyl-1,2,3,3a,3b,4,5,7,10,10a,10b,11,12,12a-tetradecahydrocyclopenta[5,6]naphtho[1,2-f]indazole-1-carbothioic S-acid; propionyl chloride; With triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;

With N'-ethyl-N,N-dimethyl-1,2-ethanediamine; In dichloromethane; for 0.166667h;