1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate

Base Information

Chemical Name:1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate
CAS No.:1229246-35-8
Molecular Formula:C₁₅H₁₈BrCl₂NO₂
Molecular Weight:395.123
Hs Code.:

Synonyms:1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate

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Chemical Property of 1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate

Chemical Property:

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Technology Process of 1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate

There total 4 articles about 1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1194490-06-6
N-[(5-bromo-2,3-dichlorophenyl)methyl]cyclopropanamine

: 1229246-35-8
1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 1229246-37-0
5-bromo-2,3-dichlorobenzaldehyde

: 1229246-35-8
1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: magnesium sulfate / dichloromethane / 20 °C

2: magnesium sulfate / dichloromethane / 20 °C

3: sodium tetrahydroborate / tetrahydrofuran; methanol / 48 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

With sodium tetrahydroborate; magnesium sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: C₁₀H₈BrCl₂N

: 1229246-35-8
1,1-dimethylethyl [(5-bromo-2,3-dichlorophenyl)methyl]cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 48 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;