4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol

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Chemical Name:4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol
CAS No.:261156-01-8
Molecular Formula:C₁₄H₁₃ClN₆S
Molecular Weight:332.816
Hs Code.:

Synonyms:4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol

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Chemical Property of 4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol

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Technology Process of 4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol

There total 3 articles about 4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 947-95-5
5-chloro-4-formyl-3-methyl-1-phenyl-1H-pyrazole

: 20939-15-5
3-methyl-4-amino-5-mercapto-1,2,4-triazole

: 261156-01-8
4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol

Guidance literature:: With sulfuric acid; In ethanol; for 1.5h; Heating;

Reference yield:

: 100-63-0
phenylhydrazine

: 261156-01-8
4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / Reflux

2.1: trichlorophosphate / 0.5 h / 0 - 10 °C

2.2: 90 - 100 °C

3.1: acetic acid / ethanol / Reflux

With acetic acid; trichlorophosphate; In ethanol; 2.1: |Vilsmeier Reaction / 2.2: |Vilsmeier Reaction;
DOI:10.1016/j.jfluchem.2016.02.004

Reference yield:

: 89-25-8
edaravone

: 261156-01-8
4-(((5-chloro-1-phenyl-3-methyl-1H-pyrazol-4-yl)methylene)amino)-5-methyl-4H-1,2,4-triazole-3-thiol

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 0.5 h / 0 - 10 °C

1.2: 90 - 100 °C

2.1: acetic acid / ethanol / Reflux

With acetic acid; trichlorophosphate; In ethanol; 1.1: |Vilsmeier Reaction / 1.2: |Vilsmeier Reaction;
DOI:10.1016/j.jfluchem.2016.02.004