benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside

Base Information

Chemical Name:benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside
CAS No.:114244-38-1
Molecular Formula:C₁₇H₂₂O₅S₂
Molecular Weight:371.483
Hs Code.:

Synonyms:benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside

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Chemical Property of benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside

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Technology Process of benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside

There total 4 articles about benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28070-06-6
benzyl-3,4-O-isopropylidene-β-D-erythro-pentoribopyranosid-2-ulose

: 114244-38-1
benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / lithium aluminium deuteride / tetrahydrofuran / 1.) 15 min., 0 deg C, 2.) 3 h. room temp.

With lithium aluminium deuteride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)86822-8

Reference yield:

: 6336-16-9
benzyl 3,4-O-isopropylidene-β-D-arabinopyranoside

: 114244-38-1
benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / chromium (VI) oxide,pyridine,acetic anhydride / CH₂Cl₂ / 0.25 h / 20 °C

2: 94 percent / lithium aluminium deuteride / tetrahydrofuran / 1.) 15 min., 0 deg C, 2.) 3 h. room temp.

With pyridine; chromium(VI) oxide; lithium aluminium deuteride; acetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(01)86822-8

Reference yield:

: 5329-50-0
(-)-benzyl β-D-arabinopyranoside

: 114244-38-1
benzyl 3,4-isopropylidene-2(R)-deuterio-2-O-<(methylthio)thiocarbonyl>-β-D-erythro-pentopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / p-toluen-sulfonic acid monohydrate / dimethylformamide / 2 h / 20 °C

2: 88 percent / chromium (VI) oxide,pyridine,acetic anhydride / CH₂Cl₂ / 0.25 h / 20 °C

3: 94 percent / lithium aluminium deuteride / tetrahydrofuran / 1.) 15 min., 0 deg C, 2.) 3 h. room temp.

With pyridine; chromium(VI) oxide; lithium aluminium deuteride; acetic anhydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)86822-8