(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))(SiMe₃)

Base Information

• Chemical Name: (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))(SiMe₃)
• CAS No.: 1013399-82-0
• Molecular Formula: C₄₅H₈₃BS₂Si₈
• Molecular Weight: 923.781

Synonyms:(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))(SiMe₃)

Chemical Property of (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))(SiMe₃)

Chemical Property:

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Technology Process of (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))(SiMe₃)

There total 1 articles about (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))(SiMe₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

chloro-trimethyl-silane (75-77-4) + (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2 (1013399-81-9) → (mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))(SiMe3) (1013399-82-0)

Guidance literature:

With MeLi; In tetrahydrofuran; diethyl ether; (Ar); soln. of MeLi in Et2O was added to soln. of B compd. in THF at 0°C; stirred at 0°C for 40 min; Me3SiCl was added; solvent removed; chromd. (SiO2 plate, hexane);

DOI:10.1021/om7008974

upstream raw materials:

chloro-trimethyl-silane

(mesityl)(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)Si(B(dithiocatecholato))2

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