triphenyltin di-t-butylphosphine

Base Information

Chemical Name:triphenyltin di-t-butylphosphine
CAS No.:74333-48-5
Molecular Formula:C₂₆H₃₃PSn
Molecular Weight:495.232
Hs Code.:

Synonyms:triphenyltin di-t-butylphosphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenyltin di-t-butylphosphine

Chemical Property:

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Technology Process of triphenyltin di-t-butylphosphine

There total 1 articles about triphenyltin di-t-butylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.2%

: 42491-34-9
di-tert-butyl(trimethylsilyl)phosphane

: 639-58-7
triphenyltin chloride

: 75-77-4
chloro-trimethyl-silane

: 74333-48-5
triphenyltin di-t-butylphosphine

Guidance literature:: In toluene; addn. of equimolar amts. of Me3SiP(t-C4H9)2 in toluene to satd. soln. of Ph3SnCl, 1h, room temp., stirred, distn., under Ar; recrystn. from pentane/toluene, -78°C; elem. anal.;
DOI:10.1016/S0022-328X(00)82878-8

Reference yield: 78.5%

: 74333-48-5
triphenyltin di-t-butylphosphine

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 74323-58-3
triphenyltin di-t-butylphosphinetricarbonylnickel

Guidance literature:: In pentane; byproducts: CO; addn. of Ni(CO)4 to soln. of Sn compd., 0°C, low press., warmed up to room temp., reaction monitored by measuring of formed CO, evapn. in vac., under Ar; recrystn. from pentane or pentane/toluene; elem. anal.;
DOI:10.1016/S0022-328X(00)82878-8