(S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol

Base Information

Chemical Name:(S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol
CAS No.:114788-08-8
Molecular Formula:C₁₄H₁₇N₃O
Molecular Weight:243.308
Hs Code.:

Synonyms:(S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol

Chemical Property:

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Technology Process of (S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol

There total 1 articles about (S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114995-10-7
(S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4.5-c>pyridine-6-carboxylic acid methyl ester

: 114788-08-8
(S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm00115a014

Reference yield:

: 114788-08-8
(S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 114788-09-9
(S)-1-Benzyl-6-(tert-butyl-dimethyl-silanyloxymethyl)-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridine

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; N,N-dimethyl-formamide; at 40 ℃; for 5h;
DOI:10.1021/jm00115a014

Reference yield:

: 114788-08-8
(S)-4,5,6,7-tetrahydro-1-(phenylmethyl)-1H-imidazo<4,5-c>pyridine-6-methanol

: 114787-63-2
1-((S)-1-Benzyl-6-hydroxymethyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-2-phenyl-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / tetrahydrofuran; dimethylformamide / 5 h / 40 °C

2: dicyclohexylcarbodiimide (DCC), hydroxybenztriazole (HOBT*H₂O) / acetonitrile / Ambient temperature

3: 2percent HF / acetonitrile / 8 h / Ambient temperature

With 1H-imidazole; hydrogen fluoride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm00115a014