C₂₁H₂₁FN₂O₂

Base Information

Chemical Name:C₂₁H₂₁FN₂O₂
CAS No.:1374109-12-2
Molecular Formula:C₂₁H₂₁FN₂O₂
Molecular Weight:352.408
Hs Code.:

C<sub>21</sub>H<sub>21</sub>FN<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₁H₂₁FN₂O₂

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Chemical Property of C₂₁H₂₁FN₂O₂

Chemical Property:

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Technology Process of C₂₁H₂₁FN₂O₂

There total 5 articles about C₂₁H₂₁FN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1374108-79-8
C₂₀H₁₉FN₂O₂

: 74-88-4
methyl iodide

: 1374109-12-2
C₂₁H₂₁FN₂O₂

Guidance literature:: C₂₀H₁₉FN₂O₂; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 0.0833333h; Cooling with ice; Inert atmosphere;

methyl iodide; for 0.166667h;

Reference yield:

: 580-15-4
6-aminoquinoline

: 1374109-12-2
C₂₁H₂₁FN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 0.5 h / 120 °C

2.1: 3-chloro-benzenecarboperoxoic acid / methanol; chloroform / 16 h / 20 °C

3.1: potassium carbonate; p-toluenesulfonyl chloride / chloroform / 3.5 h / 20 °C / Reflux

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 5.5 h / 80 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / Cooling with ice; Inert atmosphere

5.2: 0.17 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; potassium carbonate; p-toluenesulfonyl chloride; 3-chloro-benzenecarboperoxoic acid; In methanol; 1,2-dimethoxyethane; chloroform; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1374108-77-6
6-((tert-butoxycarbonyl)amino)quinoline-N-oxide

: 1374109-12-2
C₂₁H₂₁FN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; p-toluenesulfonyl chloride / chloroform / 3.5 h / 20 °C / Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 5.5 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / Cooling with ice; Inert atmosphere

3.2: 0.17 h

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; potassium carbonate; p-toluenesulfonyl chloride; In 1,2-dimethoxyethane; chloroform; water; N,N-dimethyl-formamide; mineral oil;