(2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate)

Base Information

Chemical Name:(2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate)
CAS No.:1422507-41-2
Molecular Formula:C₃₇H₄₇N₃O₈
Molecular Weight:661.795
Hs Code.:

Synonyms:(2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate)

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Technology Process of (2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate)

There total 5 articles about (2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1401468-85-6
(S)-benzyl 4-(5-((S)-4-(benzyloxy)-3-(tert-butoxycarbonylamino)-4-oxobutyl)-4-bromopyridin-3-yl)-2-(tert-butoxycarbonylamino)butanoate

: 1422507-41-2
(2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate)

Guidance literature:: With chloro-trimethyl-silane; zinc; In N,N-dimethyl-formamide; at 50 ℃; for 24h; Inert atmosphere;
DOI:10.3987/COM-12-12600

Reference yield: 39.0%

: 625-92-3
3,5-dibromopyridine

: 119768-48-8
(S)-2-((tert-butoxycarbonyl)amino)-4-iodobutyric acid benzyl ester

: 1422507-41-2
(2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate)

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; In N,N-dimethyl-formamide; at 50 ℃; for 24h;
DOI:10.3987/COM-12-12600

Reference yield: 32.0%

: 53710-18-2
3,5-diiodopyridine

: C₁₆H₂₃INO₄^(1-)*Zn⁽¹⁺⁾

: 1422507-41-2
(2S,2’S)-benzyl 4,4’-(pyridine-3,5-diyl)bis(2-(tert-butoxycarbonylamino)butanoate)

Guidance literature:: With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; In N,N-dimethyl-formamide; at 50 ℃; for 24h; Reagent/catalyst; Inert atmosphere;
DOI:10.3987/COM-12-12600