Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2

Base Information

Chemical Name:Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2
CAS No.:97690-03-4
Molecular Formula:C₅₂H₄₆Cl₂Ir₂O₂P₄
Molecular Weight:1282.18
Hs Code.:

Ir<sub>2</sub>H<sub>2</sub>Cl<sub>2</sub>(CO)2(((C<sub>6</sub>H<sub>5</sub>)2P)2CH<sub>2</sub>)2

Synonyms:Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2

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Chemical Property of Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2

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Technology Process of Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2

There total 1 articles about Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66125-35-7
IrCl(CO)(((C₆H₅)2P)2CH₂)2

: 97690-03-4
Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2

Guidance literature:: With H₂; In dichloromethane; stirring in soln. under 1 atm of H2 for 15 min, color changing from dark purple to light yellow, concg. to 5 ml under H2, hexane adding, ppt. sepg.; identified by IR and NMR spectra;

Reference yield: 90.0%

: 97690-03-4
Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2

: 97690-08-9
Ir₂H(CH₃OCOCCHCOOCH₃)Cl₂(CO)2(((C₆H₅)2P)2CH₂)2

Guidance literature:: With DMA; In dichloromethane; 1equiv of the ligand adding to a soln. of the complex under N2, color changing from pale to bright yellow, stirring for 12 h during which time a yellow ppt. appearing, Et2O adding for complete pptn., the ppt. washing with Et2O and drying under N2; identified by elem. anal., IR and NMR spectra;

Reference yield: 85.0%

: 14104-20-2
silver tetrafluoroborate

: 97690-03-4
Ir₂H₂Cl₂(CO)2(((C₆H₅)2P)2CH₂)2

: 97690-07-8
{Ir2(H)2(CO)2(μ-Cl)(bis(diphenylphosphino)methane)2}{BF4}

Guidance literature:: In tetrahydrofuran; 1 equiv of AgBF4 adding to a slurry of the complex in THF under N2, color changing to bright yellow and a yellow ppt. appe? taking to dryness under a stream of N2, extd. with CH2Cl2, filtering under N2, Et2O adding, ppt. sepg.; identified by elem. anal., IR and NMR spectra;