Technology Process of C23H36O4Si
There total 6 articles about C23H36O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
dichloromethane;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/ol102201z
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / dichloromethane / Inert atmosphere
2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / Inert atmosphere
3: tetrahydrofuran / Inert atmosphere
4: potassium hydride; Trimethylenediamine / 0 °C / Inert atmosphere
5: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere
With
1H-imidazole; oxalyl dichloride; potassium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; Trimethylenediamine; triethylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
2: Swern oxidation;
DOI:10.3762/bjoc.7.66
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium aluminium tetrahydride / diethyl ether / Inert atmosphere
2: toluene-4-sulfonic acid / dichloromethane / Inert atmosphere
3: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / Inert atmosphere
4: tetrahydrofuran / Inert atmosphere
5: potassium hydride; Trimethylenediamine / 0 °C / Inert atmosphere
6: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere
With
1H-imidazole; lithium aluminium tetrahydride; oxalyl dichloride; potassium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; Trimethylenediamine; triethylamine;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
3: Swern oxidation;
DOI:10.3762/bjoc.7.66
