3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester

Base Information

Chemical Name:3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester
CAS No.:39629-61-3
Molecular Formula:C₁₉H₂₂ClNO₂
Molecular Weight:331.842
Hs Code.:

Synonyms:3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester

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Chemical Property of 3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester

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Technology Process of 3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester

There total 5 articles about 3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 31469-16-6
1-ethoxy-1-((trimethylsilyl)oxy)-2-methylpropene

: 1613-89-4
(E)-N-benzylidene-4-chloroaniline

: 39629-61-3
3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester

Guidance literature:: With Amberlyst 15 Dry; In ethanol; at 20 ℃; for 4h;
DOI:10.1039/b106662e

Reference yield:

: 600-00-0
ethyl 2-bromoisobutyrate

: 1613-89-4
(E)-N-benzylidene-4-chloroaniline

: 39629-61-3
3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester

: 1-(4-chloro-phenyl)-3,3-dimethyl-4-phenyl-azetidin-2-one

Guidance literature:: With iodine; zinc; In 1,4-dioxane; at 20 ℃; for 0.0833333h; Title compound not separated from byproducts.; sonication;
DOI:10.1016/j.tet.2004.01.002

Reference yield:

: 100-52-7
benzaldehyde

: 39629-61-3
3-(4-Chloro-phenylamino)-2,2-dimethyl-3-phenyl-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 24 h / 20 °C

2: iodine; zinc / dioxane / 0.08 h / 20 °C / sonication

With iodine; zinc; In 1,4-dioxane; benzene; 2: Reformatsky reaction;
DOI:10.1016/j.tet.2004.01.002