4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether

Base Information

• Chemical Name: 4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether
• CAS No.: 139371-09-8
• Molecular Formula: C₂₅H₂₄O₄S₂
• Molecular Weight: 452.595
• Mol file: 139371-09-8.mol

Synonyms:4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether

Chemical Property of 4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether

There total 4 articles about 4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-bromo-2-phenylsulphinylyprop-1-ene (74338-92-4) + 4-methyl-2-(2-phenylsulfinyl-2-propenyl)phenol (139371-02-1) → 4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether (139371-09-8)

Guidance literature:

With sodium ethanolate; In ethanol;

DOI:10.1246/bcsj.64.3682

Reference yield:

p-cresol (106-44-5) → 4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether (139371-09-8)

Guidance literature:

Multi-step reaction with 4 steps

1: NaOEt / ethanol

2: 93 percent / 3 h / 110 °C

3: 80 percent / various solvent(s) / Heating

4: 90 percent / NaOEt / ethanol

With sodium ethanolate; In ethanol;

DOI:10.1246/bcsj.64.3682

Reference yield:

1-methyl-4-(2-propynyloxy)benzene (5651-90-1) → 4-methoxy-2-(2-phenylsulfinyl-2-propenyl)phenyl 2-phenylsulfinyl-2-propyl ether (139371-09-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 93 percent / 3 h / 110 °C

2: 80 percent / various solvent(s) / Heating

3: 90 percent / NaOEt / ethanol

With sodium ethanolate; In ethanol;

DOI:10.1246/bcsj.64.3682

upstream raw materials:

3-bromo-2-phenylsulphinylyprop-1-ene

4-methyl-2-(2-phenylsulfinyl-2-propenyl)phenol

p-cresol

1-methyl-4-(2-propynyloxy)benzene

Downstream raw materials:

4-methoxy-2,6-bis(2-phenylsulfinyl-2-propenyl)phenol

5-methoxy-2-methyl-7-(2-phenylsulfinyl-2-propenyl)benzofuran