12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid

Base Information

Chemical Name:12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid
CAS No.:426210-66-4
Molecular Formula:C₃₁H₅₄N₂O₆
Molecular Weight:550.78
Hs Code.:

Synonyms:12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid

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Chemical Property of 12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid

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Technology Process of 12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid

There total 4 articles about 12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 426210-64-2
12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid methyl ester

: 426210-66-4
12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid

Guidance literature:: With sodium hydroxide; for 18h; Heating;
DOI:10.1039/b005436o

Reference yield:

: 26825-95-6
methyl 12-bromododecanoate

: 426210-66-4
12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Na₂CO₃; KI / various solvent(s) / 24 h / Heating

2: 90 percent / 2N NaOH / methanol / 24 h / Heating

With sodium hydroxide; sodium carbonate; potassium iodide; In methanol;
DOI:10.1002/jhet.5570380623

Reference yield:

: 94605-71-7
7-benzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 426210-66-4
12-(16-benzyl-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl)-dodecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Na₂CO₃; KI / 24 h / Heating

2: 98 percent / aq. NaOH / 18 h / Heating

With sodium hydroxide; sodium carbonate; potassium iodide; 1: Alkylation / 2: Hydrolysis;
DOI:10.1039/b005436o