C₂₂H₁₈O₇

Base Information

Chemical Name:C₂₂H₁₈O₇
CAS No.:1446307-19-2
Molecular Formula:C₂₂H₁₈O₇
Molecular Weight:394.381
Hs Code.:

C<sub>22</sub>H<sub>18</sub>O<sub>7</sub>

Synonyms:C₂₂H₁₈O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₈O₇

Chemical Property:

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Technology Process of C₂₂H₁₈O₇

There total 9 articles about C₂₂H₁₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 58084-83-6
2',4',5,5'-tetramethoxy-2,2-dimethylpyrano<5,6-g>isoflavone

: 1446307-19-2
C₂₂H₁₈O₇

Guidance literature:: With ammonium cerium (IV) nitrate; In water; acetonitrile; at 20 ℃; for 1h; regioselective reaction; Cooling with ice;
DOI:10.1002/ejoc.201201339

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 1446307-19-2
C₂₂H₁₈O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: zinc(II) chloride; hydrogenchloride / diethyl ether / 36 h / 0 - 20 °C / Cooling with ice

1.2: 3 h / Reflux

2.1: boron trifluoride diethyl etherate; methanesulfonyl chloride / 3.83 h / 20 - 90 °C

3.1: potassium carbonate; potassium iodide; copper(l) iodide / acetone / 3 h / Inert atmosphere; Reflux

4.1: 5,5-dimethyl-1,3-cyclohexadiene / 20 h / 130 °C / Inert atmosphere

5.1: silver(l) oxide / acetone / 3 h / Reflux

6.1: ammonium cerium (IV) nitrate / acetonitrile; water / 1 h / 20 °C / Cooling with ice

With hydrogenchloride; copper(l) iodide; ammonium cerium (IV) nitrate; boron trifluoride diethyl etherate; potassium carbonate; methanesulfonyl chloride; potassium iodide; zinc(II) chloride; silver(l) oxide; In 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; water; acetone; acetonitrile; 1.1: |Houben-Hoesch Phenol Acylation / 1.2: |Houben-Hoesch Phenol Acylation / 2.1: |Vilsmeier-Haack Formylation / 4.1: |Claisen Rearrangement;
DOI:10.1002/ejoc.201201339

Reference yield:

: 38444-50-7
2,4,5-trimethoxybenzeneacetonitrile

: 1446307-19-2
C₂₂H₁₈O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: zinc(II) chloride; hydrogenchloride / diethyl ether / 36 h / 0 - 20 °C / Cooling with ice

1.2: 3 h / Reflux

2.1: boron trifluoride diethyl etherate; methanesulfonyl chloride / 3.83 h / 20 - 90 °C

3.1: potassium carbonate; potassium iodide; copper(l) iodide / acetone / 3 h / Inert atmosphere; Reflux

4.1: 5,5-dimethyl-1,3-cyclohexadiene / 20 h / 130 °C / Inert atmosphere

5.1: silver(l) oxide / acetone / 3 h / Reflux

6.1: ammonium cerium (IV) nitrate / acetonitrile; water / 1 h / 20 °C / Cooling with ice

With hydrogenchloride; copper(l) iodide; ammonium cerium (IV) nitrate; boron trifluoride diethyl etherate; potassium carbonate; methanesulfonyl chloride; potassium iodide; zinc(II) chloride; silver(l) oxide; In 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; water; acetone; acetonitrile; 1.1: |Houben-Hoesch Phenol Acylation / 1.2: |Houben-Hoesch Phenol Acylation / 2.1: |Vilsmeier-Haack Formylation / 4.1: |Claisen Rearrangement;
DOI:10.1002/ejoc.201201339