(η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt

Base Information

Chemical Name:(η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt
CAS No.:182627-86-7
Molecular Formula:C₃₄H₂₄ClCoO
Molecular Weight:543.01
Hs Code.:

Synonyms:(η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt

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Chemical Property of (η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt

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Technology Process of (η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt

There total 2 articles about (η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 79-37-8
oxalyl dichloride

: 182627-85-6
(η⁵-carboxycyclopentadienyl)(η⁴-tetraphenylcyclobutadiene)cobalt

: 182627-86-7
(η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt

Guidance literature:: In dichloromethane; N2-atmosphere; refluxing in dark overnight; solvent removal (vac.); can be recrystallized (hexane); elem. anal.;
DOI:10.1016/0022-328X(96)06381-4

Reference yield:

: 182627-85-6
C₃₄H₂₅CoO₂

: 182627-86-7
(η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 0.5h;
DOI:10.1002/chem.201302922

Reference yield: 44.0%

: 182627-86-7
(η(5)-chloroformylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt

: 7664-41-7
ammonia

: 182627-87-8
(η(5)-carbamoylcyclopentadienyl)(η(4)-tetraphenylcyclobutadiene)cobalt

Guidance literature:: In tetrahydrofuran; N2-atmosphere; stirring and bubbling NH3 at 0°C for 10 min, then stirring at 0°C for 2 h, warming to room temp.; solvent removal; can be recrystallized (Et2O/heptane); elem. anal.;
DOI:10.1016/0022-328X(96)06381-4