C₁₈H₁₇I₄NO₄

Base Information

Chemical Name:C₁₈H₁₇I₄NO₄
CAS No.:1300857-63-9
Molecular Formula:C₁₈H₁₇I₄NO₄
Molecular Weight:818.955
Hs Code.:

C<sub>18</sub>H<sub>17</sub>I<sub>4</sub>NO<sub>4</sub>

Synonyms:C₁₈H₁₇I₄NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₇I₄NO₄

Chemical Property:

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Technology Process of C₁₈H₁₇I₄NO₄

There total 9 articles about C₁₈H₁₇I₄NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14753-26-5
3-chloropropan-1-amine

: methyl 2-(4-(4-hydroxy-3,5-diiodophenoxy)-3,5-diiodophenyl)acetate

: 1300857-63-9
C₁₈H₁₇I₄NO₄

Guidance literature:: With triethylamine; In cyclopentyl methyl ether; for 3h; Reflux;

Reference yield:

: 83799-60-4
(4-hydroxy-3,5-dinitro-phenyl)-acetic acid ethyl ester

: 1300857-63-9
C₁₈H₁₇I₄NO₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine; p-toluenesulfonyl chloride / 0.5 h / 95 - 100 °C

1.2: 2 h / 125 °C / Inert atmosphere

2.1: hydrogen / 5% Pd-CaCO3 / ethanol

3.1: sodium nitrite; sulfuric acid; acetic acid / 1.75 h / 0 °C

3.2: 1 h / 20 °C

4.1: phosphorus; hydrogen iodide; acetic acid / 1 h / Reflux

5.1: iodine; ammonia / methanol

6.1: thionyl chloride / 48 h / Reflux

7.1: triethylamine / cyclopentyl methyl ether / 3 h / Reflux

With pyridine; phosphorus; thionyl chloride; sulfuric acid; ammonia; hydrogen iodide; hydrogen; iodine; acetic acid; triethylamine; p-toluenesulfonyl chloride; sodium nitrite; 5% Pd-CaCO3; In methanol; ethanol; cyclopentyl methyl ether;

Reference yield:

: 861065-72-7
[4-(4-methoxy-phenoxy)-3,5-dinitro-phenyl]-acetic acid ethyl ester

: 1300857-63-9
C₁₈H₁₇I₄NO₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen / 5% Pd-CaCO3 / ethanol

2.1: sodium nitrite; sulfuric acid; acetic acid / 1.75 h / 0 °C

2.2: 1 h / 20 °C

3.1: phosphorus; hydrogen iodide; acetic acid / 1 h / Reflux

4.1: iodine; ammonia / methanol

5.1: thionyl chloride / 48 h / Reflux

6.1: triethylamine / cyclopentyl methyl ether / 3 h / Reflux

With phosphorus; thionyl chloride; sulfuric acid; ammonia; hydrogen iodide; hydrogen; iodine; acetic acid; triethylamine; sodium nitrite; 5% Pd-CaCO3; In methanol; ethanol; cyclopentyl methyl ether;