8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene

Base Information

• Chemical Name: 8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene
• CAS No.: 64724-54-5
• Molecular Formula: C₁₄H₅F₁₂N₃S
• Molecular Weight: 475.261

Synonyms:8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene

Chemical Property of 8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene

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Technology Process of 8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene

There total 3 articles about 8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.0^2,4]oct-6-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.6%

1,2,3,4-tetrakis(trifluoromethyl)-5-thiabicyclo{2.1.0}pent-2-ene (39091-73-1) + Phenyl azide (622-37-7) → 8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.02,4]oct-6-ene (64724-54-5)

Guidance literature:

In dichloromethane; for 72h; Product distribution; Ambient temperature; react. with various azides;

DOI:10.1021/jo01303a009

Reference yield:

→ 8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.02,4]oct-6-ene (64724-54-5)

Guidance literature:

Thiophen II, Phenylazid;

Reference yield:

→ 8-phenyl-1,2,4,5-tetrakis-trifluoromethyl-(1rH,2tH,4tH,5cH)-3-thia-6,7,8-triaza-tricyclo[3.3.0.02,4]oct-6-ene (64724-54-5)

Guidance literature:

(1)/(2a);

DOI:10.1021/ja00464a040

upstream raw materials:

1,2,3,4-tetrakis(trifluoromethyl)-5-thiabicyclo{2.1.0}pent-2-ene

Phenyl azide

Downstream raw materials:

6-phenyl-1,2,4,5-tetrakis(trifluoromethyl)-6-aza-3-thiatricyclo<3.1.0.0^2,4>hexane

Phenyl-[2,2,2-trifluoro-1-(2,3,4-tris-trifluoromethyl-2H-thiet-2-yl)-eth-(E)-ylidene]-amine

4-phenyl-1,5,6,7-tetrakis(trifluoromethyl)-2,3,4-triazabicyclo<3.2.0>hepta-2,6-diene

[1-[3-(1-Diazo-2,2,2-trifluoro-ethyl)-2,3-bis-trifluoromethyl-thiiranyl]-2,2,2-trifluoro-eth-(E)-ylidene]-phenyl-amine

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