4-Chlorobenzoyl chloride phenyl hydrazone

Base Information

• Chemical Name: 4-Chlorobenzoyl chloride phenyl hydrazone
• CAS No.: 36590-52-0
• Molecular Formula: C13H10 Cl2 N2
• Molecular Weight: 265.142
• Hs Code.: 2928000090
• ChEMBL ID: CHEMBL150895
• Mol file: 36590-52-0.mol

Synonyms:BRN 0959323;4-Chlorobenzoyl chloride phenyl hydrazone;36590-52-0;BENZOYL CHLORIDE, p-CHLORO-, PHENYLHYDRAZONE;Benzene carbohydrazonoyl chloride, 4-chloro-N-phenyl-;CHEMBL150895;SCHEMBL8131896;Benzoyl chloride p-chloro-,phenylhydrazone;LS-42597;BENZOYL CHLORIDE P-CHLORO-, PHENYLHYDRAZONE

Chemical Property of 4-Chlorobenzoyl chloride phenyl hydrazone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 369.16°C at 760 mmHg
• Flash Point: 177.062°C
• PSA: 24.39000
• Density: 1.245g/cm³
• LogP: 4.42550
• XLogP3: 5.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 264.0221037
• Heavy Atom Count: 17
• Complexity: 254

Purity/Quality:

99% ^*data from raw suppliers

4-CHLORO-N-PHENYLBENZENECARBOHYDRAZONOYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)NN=C(C2=CC=C(C=C2)Cl)Cl
• Isomeric SMILES: C1=CC=C(C=C1)N/N=C(/C2=CC=C(C=C2)Cl)\Cl

Technology Process of 4-Chlorobenzoyl chloride phenyl hydrazone

There total 16 articles about 4-Chlorobenzoyl chloride phenyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2-(4-Chlorbenzoyl)-1-phenylhydrazid (15089-07-3) → (Z)-1-[chloro(4-chlorophenyl)methylene]-2-phenylhydrazine (36590-52-0)

Guidance literature:

With tetrachloromethane; acetic acid; triphenylphosphine; In acetonitrile; for 20h;

DOI:10.1134/S107036321403030X

Reference yield:

N-(4-chlorobenzylidene)-N'-phenylhydrazine (2829-26-7) → N-phenyl-p-chlorobenzohydrazonoyl chloride (36590-52-0)

Guidance literature:

With N-chloro-succinimide; dimethylsulfide; In dichloromethane;

DOI:10.1055/s-0030-1258117

Reference yield:

2-(4-Chlorbenzoyl)-1-phenylhydrazid (15089-07-3) → N-phenyl-p-chlorobenzohydrazonoyl chloride (36590-52-0)

Guidance literature:

With tetrachloromethane; triphenylphosphine; In acetonitrile; at 20 ℃;

DOI:10.1111/j.1747-0285.2010.00948.x

upstream raw materials:

N-(4-chlorobenzylidene)-N'-phenylhydrazine

2-(4-Chlorbenzoyl)-1-phenylhydrazid

4-chlorobenzaldehyde

phenylhydrazine

Downstream raw materials:

3-(4-chloro-phenyl)-1-phenyl-3a,6a-dihydro-1H-furo[3,2-c]pyrazole

3-(4-chloro-phenyl)-1-phenyl-(3ar,8bc)-3a,8b-dihydro-1H-benzo[4,5]furo[3,2-c]pyrazole

3-(4-Chlorphenyl)-1,8a-dihydro-1-phenyl<1,2,4>triazolo<4,3-a>pyridin

3-(4-Chloro-phenyl)-1-phenyl-1H-pyrazolo[3,4-b]pyrazine

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