2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid

Base Information

Chemical Name:2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid
CAS No.:1333127-11-9
Molecular Formula:C₁₅H₁₄F₆N₂O₅
Molecular Weight:416.277
Hs Code.:

Synonyms:2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid

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Chemical Property of 2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid

Chemical Property:

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Technology Process of 2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid

There total 4 articles about 2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65-49-6
4-Aminosalicylic acid

: 1333127-11-9
2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 24 h

2.1: potassium carbonate / 1 h / 110 °C

3.1: hydrogenchloride / ethanol; water / 2 h

4.1: zinc; sodium hydroxide / water / 4 h / 60 °C

4.2: pH 4 - 5

5.1: sodium hydroxide; water / ethanol / 10 h / 100 °C / Sealed ampoule

5.2: pH 8 - 9

6.1: 1 h

With hydrogenchloride; water; potassium carbonate; sodium hydroxide; zinc; In 1,4-dioxane; ethanol; water;

Reference yield:

: 184033-42-9
4-[(tert-butoxycarbonyl)amino]-2-hydroxybenzoic acid

: 1333127-11-9
2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / 1 h / 110 °C

2.1: hydrogenchloride / ethanol; water / 2 h

3.1: zinc; sodium hydroxide / water / 4 h / 60 °C

3.2: pH 4 - 5

4.1: sodium hydroxide; water / ethanol / 10 h / 100 °C / Sealed ampoule

4.2: pH 8 - 9

5.1: 1 h

With hydrogenchloride; water; potassium carbonate; sodium hydroxide; zinc; In ethanol; water;

Reference yield:

: 1333127-08-4
2-[3-(acetylamino)propoxy]-4-aminobenzoic acid

: 1333127-11-9
2-[3-(trifluoroacetylamino)propoxy]-4-[trifluoroacetyl-(methyl)amino]benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc; sodium hydroxide / water / 4 h / 60 °C

1.2: pH 4 - 5

2.1: sodium hydroxide; water / ethanol / 10 h / 100 °C / Sealed ampoule

2.2: pH 8 - 9

3.1: 1 h

With water; sodium hydroxide; zinc; In ethanol; water;